Analysis of essential oil of Nardostachys chinensis Batal by GC-MS combined with chemometric techniques

Czasopismo : Acta Chromatographica
Tytuł artykułu : Analysis of essential oil of Nardostachys chinensis Batal by GC-MS combined with chemometric techniques

Autorzy :
Gwarda, R. Ł.
Medical University of Lublin Department of Physical Chemistry, Chair of Chemistry 4a Chodźki Street 20-093 Lublin Poland, radoslaw.gwarda@umlub.pl,,
Tomczyszyn, A.
University of Warsaw Faculty of Chemistry 1 Pasteura Street 02-093 Warsaw Poland,
Misicka, A.
University of Warsaw Faculty of Chemistry 1 Pasteura Street 02-093 Warsaw Poland,
Dzido, T. H.
Medical University of Lublin Department of Physical Chemistry, Chair of Chemistry 4a Chodźki Street 20-093 Lublin Poland,
Xue, X. D.
Yunnan Normal University Department of Chemistry Kunming 650092 P.R. China,
Zhang, M.
East China Normal University Department of Chemistry Shanghai 200241 P.R. China,
Xie, S. M.
Yunnan Normal University Department of Chemistry Kunming 650092 P.R. China,
Yuan, L. M.
Yunnan Normal University Department of Chemistry Kunming 650092 P.R. China, yuan_limingpd@yahoo.com.cn,
Matta, M. K.
Jawaharlal Nehru Technological University University College of Pharmaceutical Sciences Hyderabad 500 085 India,
Pilli, N. R.
Jawaharlal Nehru Technological University University College of Pharmaceutical Sciences Hyderabad 500 085 India,
Rao, J. V. L. N. S.
Yalamarty College of Pharmaceutical Sciences Visakhapatnam 530 052 India, jvlnsrao@rediffmail.com,
Abdelhay, M. H.
University of Alexandria Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy Elmessalah, Alexandria 21521 Egypt,
Gazy, A. A.
University of Alexandria Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy Elmessalah, Alexandria 21521 Egypt,
Shaalan, R. A.
rasha_shaalan@yahoo.com,
Ashour, H. K.
University of Alexandria Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy Elmessalah, Alexandria 21521 Egypt,
Krasucka, D.
National Veterinary Research Institute — National Research Institute Department of Veterinary Pharmacy Al. Partyzantów 57 24-100 Pulawy Poland,
Kowalski, C. J.
University of Life Sciences in Lublin Department of Pharmacology, Faculty of Veterinary Medicine Akademicka 12 20-033 Lublin Poland,
Osypiuk, M.
University of Life Sciences in Lublin Department of Pharmacology, Faculty of Veterinary Medicine Akademicka 12 20-033 Lublin Poland, monika.osypiuk@up.lublin.pl,
Opielak, G.
Medical University School of Lublin Human Anatomy Department Jaczewskiego 4 20-090 Lublin Poland,
Mahgoub, H.
King Abdulaziz University Department of Pharmaceutical Chemistry, Faculty of Pharmacy Jeddah Saudi Arabia, hodamahgoub@yahoo.com,
Hanafy, A.
King Abdulaziz University Department of Pharmacology and Toxicology, Faculty of Pharmacy Jeddah Saudi Arabia,
Bamane, F. H.
King Abdulaziz University Department of Biochemistry, Faculty of Medicine Jeddah Saudi Arabia,
Radwan, A. E.
University of Alexandria Department of Biotechnology, Institute of Graduate Studies and Research Alexandria Egypt,
Wen, C.
Wenzhou Medical College Laboratory Animal Centre Wenzhou 325035 China,
Zhang, Q.
Shanghai Institute of Pharmaceutical Industry Shanghai 200437 China,
He, Y.
Wenzhou Medical College Laboratory Animal Centre Wenzhou 325035 China,
Deng, M.
Wenzhou Medical College Laboratory Animal Centre Wenzhou 325035 China,
Wang, X.
Wenzhou Medical College Laboratory Animal Centre Wenzhou 325035 China,
Ma, J.
Wenzhou Medical College Function Experiment Teaching Center Wenzhou 325035 China, jianshema@gmail.com,
Wang, Y.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Wang, M. J.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Li, J.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Yao, S. C.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Xue, J.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Zou, W. B.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China,
Hu, C.
National Institutes for Food and Drug control (NIFDC) Beijing 100050 P.R. China, hucq@nicpbp.org.cn,
Idris, A. M.
King Khalid University Department of Chemistry, College of Science Abha Saudi Arabia, abubakridris@hotmail.com,
Alnajjar, A. O.
King Faisal University Department of Chemistry, College of Science Hofuf Saudi Arabia,
Vichapong, J.
Khon Kaen University Materials Chemistry Research Unit, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science Khon Kaen 40002 Thailand,
Burakham, R.
Khon Kaen University Materials Chemistry Research Unit, Department of Chemistry and Center of Excellence for Innovation in Chemistry, Faculty of Science Khon Kaen 40002 Thailand, rodjbu@kku.ac.th,
Srivastava, P.
Agharkar Research Institute Chemistry Group, Animal Science Division G. G. Agarkar Road Pune 411004 India, psri94@yahoo.com,
Raut, H. N.
Agharkar Research Institute Chemistry Group, Animal Science Division G. G. Agarkar Road Pune 411004 India,
Puntambekar, H. M.
Agharkar Research Institute Chemistry Group, Animal Science Division G. G. Agarkar Road Pune 411004 India,
Desai, A. C.
Indian Drug Research Association and Laboratory Drug Analysis 561/B, Shivajinagar Pune 411005 India,
Wang, F.
Central South University Xiangya Hospital Changsha Hunan 410008 China,
Liu, S.
Central South University Xiangya Hospital Changsha Hunan 410008 China, liushao999@hotmail.com,
Luo, M. Y.
Shanghai Medical College of Fudan University Shanghai 200032 China,
Qin, Y.
Jiangsu Shenlong Pharmaceutical Co., Ltd. Yanchen Jiangsu 224200 China,
Lei, P.
Central South University Xiangya Hospital Changsha Hunan 410008 China,
Liu, Y. H.
Central South University Xiangya Hospital Changsha Hunan 410008 China,
Liang, Y. Z.
Central South University College of Chemistry and Chemical Engineering Changsha Hunan 410083 China,
Abstrakty : The essential oil extracted from Nardostachys chinensis Batal (NCB) was analyzed by gas chromatography-mass spectrometry (GC-MS) combined with two chemometric resolution methods (CRM), heuristic evolving latent projections (HELP), and selective ion analysis (SIA). Qualitative analysis was performed by comparing the obtained pure mass spectra with those in National Institute of Standards and Technology (NIST) mass spectra database. Identification of some compounds was assisted by comparison of programmed temperature retention indices (PTRIs). The quantitative results were obtained by overall volume integration (OVI). A total of 69 compounds in the essential oil of N. chinensis Batal were identified, accounting for 93.98% of the total content. The major compounds were (−)-spathulenol, epiglobulol, trans-longipinocarveol, and patchouli alcohol which contribute to the antimicrobial and antioxidant activity. The results showed that the efficiency and reliability were greatly improved by use of chemometric techniques and programmed temperature retention index as assistants of GC-MS in identification of the plant essential oil.

Słowa kluczowe : Nardostachys chinensis Batal, essential oil, gas chromatography-mass spectrometry, heuristic evolving latent projections, selective ion analysis,
Wydawnictwo : University of Silesia in Katowice
Rocznik : 2015
Numer : Vol. 27, no. 1
Strony : 157 – 175
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DOI :
Cytuj : Gwarda, R. Ł. ,Tomczyszyn, A. ,Misicka, A. ,Dzido, T. H. ,Xue, X. D. ,Zhang, M. ,Xie, S. M. ,Yuan, L. M. ,Matta, M. K. ,Pilli, N. R. ,Rao, J. V. L. N. S. ,Abdelhay, M. H. ,Gazy, A. A. ,Shaalan, R. A. ,Ashour, H. K. ,Krasucka, D. ,Kowalski, C. J. ,Osypiuk, M. ,Opielak, G. ,Mahgoub, H. ,Hanafy, A. ,Bamane, F. H. ,Radwan, A. E. ,Wen, C. ,Zhang, Q. ,He, Y. ,Deng, M. ,Wang, X. ,Ma, J. ,Wang, Y. ,Wang, M. J. ,Li, J. ,Yao, S. C. ,Xue, J. ,Zou, W. B. ,Hu, C. ,Idris, A. M. ,Alnajjar, A. O. ,Vichapong, J. ,Burakham, R. ,Srivastava, P. ,Raut, H. N. ,Puntambekar, H. M. ,Desai, A. C. ,Wang, F. ,Liu, S. ,Luo, M. Y. ,Qin, Y. ,Lei, P. ,Liu, Y. H. ,Liang, Y. Z. , Analysis of essential oil of Nardostachys chinensis Batal by GC-MS combined with chemometric techniques. Acta Chromatographica Vol. 27, no. 1/2015
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