Multiple compounds determination and fingerprint analysis of Agrimonia pilosa Ledeb by high-performance liquid chromatography

Czasopismo : Acta Chromatographica
Tytuł artykułu : Multiple compounds determination and fingerprint analysis of Agrimonia pilosa Ledeb by high-performance liquid chromatography

Autorzy :
Komsta, Ł.
Medical University of Lublin Chair and Department of Medicinal Chemistry, Faculty of Pharmacy Jaczewskiego 4 20-090 Lublin Poland, lukasz.komsta@am.lublin.pl,
Gowin, E.
Medical University of Lublin Chair and Department of Medicinal Chemistry, Faculty of Pharmacy Jaczewskiego 4 20-090 Lublin Poland,
Djordjević Filijović, N.
Hemofarm AD Vrsac Serbia,
Pavlović, A.
Hemofarm AD Vrsac Serbia,
Nikolić, K.
University of Belgrade, Faculty of Pharmacy Department of Pharmaceutical Chemistry Vojvode Stepe 450 PO Box 146 11000 Belgrade Serbia,
Agbaba, D.
University of Belgrade, Faculty of Pharmacy Department of Pharmaceutical Chemistry Vojvode Stepe 450 PO Box 146 11000 Belgrade Serbia, danica@pharmacy.bg.ac.rs,
Sawant, S.
Sinhgad Technical Education Society’s Smt. Kashibai Navale College of Pharmacy, Kondhwa (Bk.) Pune 411 048 Maharashtra India, sawant99@rediffmail.com,
Barge, V.
PDEA’s Seth Govind Raghunath Sable College of Pharmacy Saswad, Tal-Purandar, Dist-Pune 412301 Maharashtra India,
Tiwari, R.
School of Pharmacy and Technology Department of Pharmaceutical Chemistry, SVKM’s NMIMS Management Shirpur Dist. Dhule 425405 Maharashtra India, ravisun4@rediffmail.com,
Bonde, C.
School of Pharmacy and Technology Department of Pharmaceutical Chemistry, SVKM’s NMIMS Management Shirpur Dist. Dhule 425405 Maharashtra India,
Bothara, K.
Sinhgad Institute of Pharmacy Department of Pharmaceutical Chemistry Narhe Road Pune 410041 Maharashtra India,
Nawaz, M.
United Arab Emirates University Department of Chemistry Al-Ain 17551 UAE, nawwaz@gmail.com,
Arayne, M. S.
University of Karachi Department of Chemistry Karachi 75270 Pakistan,
Sultana, N.
University of Karachi Research Institute of Pharmaceutical Sciences, Department of Pharmaceutical Chemistry, Faculty of Pharmacy Karachi 75270 Pakistan,
Haider, A.
University of Karachi Department of Chemistry Karachi 75270 Pakistan,
Hisaindee, S.
United Arab Emirates University Department of Chemistry Al-Ain 17551 UAE,
Youssef, R. M.
University of Alexandria Faculty of Pharmacy, Department of Pharmaceutical Analytical Chemistry El-Messalah, Alexandria 21521 Egypt, rmmy1973@yahoo.com,
Malesevic, M.
Medicines and Medical Devices Agency of Serbia Vojvode Stepe 458 11 152 Belgrade Serbia,
Zivanovic, L.
University of Belgrade Faculty of Pharmacy, Department of Drug Analysis Vojvode Stepe 450 11 152 Belgrade Serbia, ljzivan@pharmacy.bg.ac.rs,
Protic, A.
University of Belgrade Faculty of Pharmacy, Department of Drug Analysis Vojvode Stepe 450 11 152 Belgrade Serbia,
Radisic, M.
University of Belgrade Faculty of Technology and Metallurgy, Department of Analytical Chemistry 11000 Belgrade Serbia,
Lausevic, M.
University of Belgrade Faculty of Technology and Metallurgy, Department of Analytical Chemistry 11000 Belgrade Serbia,
Jovic, Z.
Medicines and Medical Devices Agency of Serbia Vojvode Stepe 458 11 152 Belgrade Serbia,
Jóźwiak, A.
Department of Inorganic Chemistry Medical University of Lublin 20-093 Lublin Poland,
Jóźwiak, G.
Department of Inorganic Chemistry Medical University of Lublin 20-093 Lublin Poland,
Waksmundzka-Hajnos, M.
Department of Inorganic Chemistry Medical University of Lublin 20-093 Lublin Poland, monika.hajnos@am.lublin.pl,
Djapic, N.
Mihajlo Pupin Djure Djakovica bb 23000 Zrenjanin Serbia, ninadjapic@yahoo.com,
Lv, X. H.
Beijing University of Chemical Technology State Key Laboratory of Chemical Resource Engineering Beijing 100029 China,
Kuang, P. Q.
Beijing University of Chemical Technology State Key Laboratory of Chemical Resource Engineering Beijing 100029 China,
Yuan, Q. P.
Beijing University of Chemical Technology State Key Laboratory of Chemical Resource Engineering Beijing 100029 China, yuanqp@mail.buct.edu.cn,
Liang, H.
Beijing University of Chemical Technology State Key Laboratory of Chemical Resource Engineering Beijing 100029 China,
Zheng, G. Q.
Beijing University of Chemical Technology State Key Laboratory of Chemical Resource Engineering Beijing 100029 China,
Wang, Y.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China,
Yin, L.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China,
Lv, G.
Central Laboratory of Dalian Medical University 9 Western Lvshun South Road Dalian 116044 China,
Xu, Y.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China,
Xu, L.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China,
Qi, Y.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China,
Zheng, L.
The First Affiliated Hospital of Dalian Medical University Dalian China, Zheng_112009@126.com,
Peng, J.
Dalian Medical University College of Pharmacy 9 Western Lvshun South Road Dalian 116044 China, jinyongpeng2008@126.com,
Abstrakty : In the present paper, a simple and reliable high-performance liquid chromatography-diode array detection (HPLC-DAD) method was developed both for quantitative determination and fingerprint analysis of Agrimonia pilosa Ledeb for quality control. Under the optimized HPLC conditions, seven bioactive compounds including rutin, quercetin-3-rhamnoside, luteoloside, tiliroside, apigenin, kaempferol, and agrimonolide were determined simultaneously. For fingerprint analysis, 11 common peaks were selected as the characteristic peaks to evaluate the similarities of 16 different samples collected from different origins in China. Besides, hierarchical cluster analysis (HCA) was also performed to evaluate the variation of the raw materials. This is the first report of using a simple method for quality control of A. pilosa Ledeb through multi-component determination and chromatographic fingerprint analysis to the best of our knowledge.

Słowa kluczowe : Agrimonia pilosa Ledeb, HPLC-DAD, hierarchical cluster analysis, quality control, fingerprint analysis,
Wydawnictwo : University of Silesia in Katowice
Rocznik : 2014
Numer : Vol. 26, no. 1
Strony : 137 – 156
Bibliografia : 1 State Pharmacopoeia Commission, Pharmacopoeia of the People’s Republic of China, China Medical Science and Technology Press, Beijing, China, 2010.
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DOI :
Cytuj : Komsta, Ł. ,Gowin, E. ,Djordjević Filijović, N. ,Pavlović, A. ,Nikolić, K. ,Agbaba, D. ,Sawant, S. ,Barge, V. ,Tiwari, R. ,Bonde, C. ,Bothara, K. ,Nawaz, M. ,Arayne, M. S. ,Sultana, N. ,Haider, A. ,Hisaindee, S. ,Youssef, R. M. ,Malesevic, M. ,Zivanovic, L. ,Protic, A. ,Radisic, M. ,Lausevic, M. ,Jovic, Z. ,Jóźwiak, A. ,Jóźwiak, G. ,Waksmundzka-Hajnos, M. ,Djapic, N. ,Lv, X. H. ,Kuang, P. Q. ,Yuan, Q. P. ,Liang, H. ,Zheng, G. Q. ,Wang, Y. ,Yin, L. ,Lv, G. ,Xu, Y. ,Xu, L. ,Qi, Y. ,Zheng, L. ,Peng, J. , Multiple compounds determination and fingerprint analysis of Agrimonia pilosa Ledeb by high-performance liquid chromatography. Acta Chromatographica Vol. 26, no. 1/2014
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