Simultaneous determination of gallic acid, protocatechuic acid, catechin, epicatechin, quercetin and kaempferol in Chinese chestnut (Castanea mollissima blume) kernel by high-performance liquid chromatography with diode array detection

Czasopismo : Acta Chromatographica
Tytuł artykułu : Simultaneous determination of gallic acid, protocatechuic acid, catechin, epicatechin, quercetin and kaempferol in Chinese chestnut (Castanea mollissima blume) kernel by high-performance liquid chromatography with diode array detection

Autorzy :
Fatemi, M. H.
University of Mazandaran Faculty of Chemistry Babolsar Iran,
Hadjmohammadi, M. R.
University of Mazandaran Faculty of Chemistry Babolsar Iran, hdjmr@umz.ac.ir,
Shakeri, P.
University of Mazandaran Faculty of Chemistry Babolsar Iran,
Bhushan, R.
Indian Institute of Technology Roorkee Department of Chemistry Roorkee 247667 India, rbushfcy@iitr.ernet.in,
Lal, M.
Indian Institute of Technology Roorkee Department of Chemistry Roorkee 247667 India,
Thomas, S.
Jubilant Life Sciences Ltd. Analytical Research Department R&D Centre, C-26, Sector-59 Noida Uttar Pradesh 201 301 India, saji_thomas@jubl.com,
Paul, S. K.
Jubilant Life Sciences Ltd. Analytical Research Department R&D Centre, C-26, Sector-59 Noida Uttar Pradesh 201 301 India,
Agarwal, A.
Jubilant Life Sciences Ltd. Analytical Research Department R&D Centre, C-26, Sector-59 Noida Uttar Pradesh 201 301 India,
Mathela, C. S.
Kumaun University Department of Chemistry DSB Campus Nainital Uttarakhand 263 001 India,
Elgizawy, S. M.
Assuit University Analytical Chemistry Department, Faculty of Pharmacy 71515 Assuit Egypt,
Hassan, N. Y.
Cairo University Analytical Chemistry Department, Faculty of Pharmacy Kasr-El Aini Street 11562 Cairo Egypt,
Lotfy, H. M.
Cairo University Analytical Chemistry Department, Faculty of Pharmacy Kasr-El Aini Street 11562 Cairo Egypt,
Saleh, S. S.
October University for Modern Sciences and Arts (MSA) Analytical Chemistry Department, Faculty of Pharmacy 11787 6th October City Egypt, drsarahsalah@gmail.com,
Shakya, A.
Al-Ahliyya Amman University Faculty of Pharmacy and Medical Sciences PO Box 263 Amman 19328 Jordan, ashokshakya@hotmail.com,
Arafat, T.
Petra University Faculty of Pharmacy PO Box 961343 Amman Jordan,
Hakooz, N. M.
Zarqa University Faculty of Pharmacy Zarqa 13132 Jordan,
Abuawwad, A. N.
Jordan Center for Pharmaceutical Research PO Box 950435 Amman 11495 Jordan,
Al-Hroub, H.
Jordan Center for Pharmaceutical Research PO Box 950435 Amman 11495 Jordan,
Melhim, M.
Jordan Center for Pharmaceutical Research PO Box 950435 Amman 11495 Jordan,
Haliński, Ł.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland, lukaszh@chem.univ.gda.pl,
Śmigiel, D.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland,
Czerwicka, M.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland,
Paszkiewicz, M.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland,
Kumirska, J.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland,
Stepnowski, P.
University of Gdańsk Department of Environmental Analysis, Institute for Environmental and Human Health Protection, Faculty of Chemistry Wita Stwosza 63 80-952 Gdańsk Poland,
Odeh, I.
Al-Quds University Chemistry and Chemical Technology Department P.O. Box 20002 Abu-Deis Palestine,
Abu-Lafi, S.
Al-Quds University Faculty of Pharmacy P.O. Box 20002 Abu-Deis Palestine, sabulafi@science.alquds.edu,
Al-Najjar, I.
Al-Quds University Chemistry and Chemical Technology Department P.O. Box 20002 Abu-Deis Palestine,
Znini, M.
University My Ismail Laboratoire des Substances Naturelles & Synthèse et Dynamique Moléculaire, Faculté des Sciences et Techniques Errachidia Morocco,
Majidi, L.
University My Ismail Laboratoire des Substances Naturelles & Synthèse et Dynamique Moléculaire, Faculté des Sciences et Techniques Errachidia Morocco, lmajidi@yahoo.fr,,
Desjobert, J. M.
Université de Corse UMR CNRS 6134, Laboratoire de Chimie des Produits Naturels, Faculté des Sciences et Techniques Corse France,
Paolini, J.
Université de Corse UMR CNRS 6134, Laboratoire de Chimie des Produits Naturels, Faculté des Sciences et Techniques Corse France,
Costa, J.
Université de Corse UMR CNRS 6134, Laboratoire de Chimie des Produits Naturels, Faculté des Sciences et Techniques Corse France,
Xie, J.
Beijing University of Chinese Medicine School of Chinese Materia Medica Beijing 100102 China,
Zhang, Y.
Tianjin University of Commerce Department of Pharmaceutical Engineering Tianjin 300134 China,
Wang, W.
Beijing University of Chinese Medicine School of Chinese Materia Medica Beijing 100102 China, wwq57@126.com,
Hou, J.
Beijing University of Chinese Medicine School of Chinese Materia Medica Beijing 100102 China,
Zhu, M.
The First Affiliated Hospital of Nanjing University of Chinese Medicine West Phoenix Street, 150-1 210036 Nanjing China,
Duan, J.
Nanjing University of Chinese Medicine Jiangsu Key Laboratory for High Technology Research of TCM Formulae Xianlin Road 138 210023 Nanjing China,
Tang, Y. P.
Nanjing University of Chinese Medicine Jiangsu Key Laboratory for High Technology Research of TCM Formulae Xianlin Road 138 210023 Nanjing China,
Guo, J. M.
Nanjing University of Chinese Medicine Jiangsu Key Laboratory for High Technology Research of TCM Formulae Xianlin Road 138 210023 Nanjing China,
Shang, E. X.
Nanjing University of Chinese Medicine Jiangsu Key Laboratory for High Technology Research of TCM Formulae Xianlin Road 138 210023 Nanjing China,
Zhu, Z. H.
Nanjing University of Chinese Medicine Jiangsu Key Laboratory for High Technology Research of TCM Formulae Xianlin Road 138 210023 Nanjing China, zhumin0902@163.com,
Wang, T.
Hebei Normal University of Science and Technology Hebei Chestnut Engineering Technology Research Center Qinhuangdao, Hebei 066600 China, trueyeoman2008@yahoo.com.cn,
Yang, Y. D.
Hebei Normal University of Science and Technology Hebei Chestnut Engineering Technology Research Center Qinhuangdao, Hebei 066600 China,
Du, B.
Hebei Normal University of Science and Technology Hebei Chestnut Engineering Technology Research Center Qinhuangdao, Hebei 066600 China, bindufood@yahoo.com.cn,
Yu, S.
Hebei Normal University of Science and Technology Hebei Chestnut Engineering Technology Research Center Qinhuangdao, Hebei 066600 China,
Hou, W. L.
Hebei Normal University of Science and Technology Hebei Chestnut Engineering Technology Research Center Qinhuangdao, Hebei 066600 China,
Abstrakty : Chestnut exhibits anti-inflammatory, styptic, anti-diarrhea, and analgestic effects as a traditional Chinese medicine. There is increasing evidence that shows that the consumption of chestnuts has become more important in human nutrition due to the health benefits provided by the antioxidants. The phenolic compounds are responsible for major bioactivities, such as anti-tumor and anti-oxidation. A high-performance liquid chromatography (HPLC) method with diode array detection (DAD) was established for the simultaneous determination of six phenolic compounds (gallic acid, GA; protocatechuic acid, PR; catechin, CA; epicatechin, EP; quercetin, QU; kaempferol, KA) in Chinese chestnut (Castanea mollissima blume) kernel. The sample followed by separation on Eclipse XDB-C18 column (150 × 4.6 mm, id., 5 μm) with gradient elution of methanol-1.0% acetate acid solution as a mobile phase, at a temperature of 30°C, under the ratio of 1.2 mL min-1, with 5 μL injection volume, and multi-wavelength synthesis was used with DAD. The correlation coefficients were larger than 0.999, the recoveries were 97.58% for GA, 100.41% for PA, 96.23% for CA, 101.38% for QU, 99.15% for EP, and 98.60% for KA, relative standard deviation (RSD) were 1.04% for GA, 1.21% for PA, 1.09% for CA, 1.19% for QU, 1.06% for EP, and 1.20% for KA. This method was applied for the determination of phenolics in chestnut kernel and was found to be fast, sensitive, and suitable.

Słowa kluczowe : Chinese chestnut (Castanea mollissima blume) kernel, gallic acid, protocatechuic acid, catechin, epicatechin, quercetin, kaempferol, HPLC-DAD,
Wydawnictwo : University of Silesia in Katowice
Rocznik : 2014
Numer : Vol. 26, no. 3
Strony : 539 – 550
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DOI :
Cytuj : Fatemi, M. H. ,Hadjmohammadi, M. R. ,Shakeri, P. ,Bhushan, R. ,Lal, M. ,Thomas, S. ,Paul, S. K. ,Agarwal, A. ,Mathela, C. S. ,Elgizawy, S. M. ,Hassan, N. Y. ,Lotfy, H. M. ,Saleh, S. S. ,Shakya, A. ,Arafat, T. ,Hakooz, N. M. ,Abuawwad, A. N. ,Al-Hroub, H. ,Melhim, M. ,Haliński, Ł. ,Śmigiel, D. ,Czerwicka, M. ,Paszkiewicz, M. ,Kumirska, J. ,Stepnowski, P. ,Odeh, I. ,Abu-Lafi, S. ,Al-Najjar, I. ,Znini, M. ,Majidi, L. ,Desjobert, J. M. ,Paolini, J. ,Costa, J. ,Xie, J. ,Zhang, Y. ,Wang, W. ,Hou, J. ,Zhu, M. ,Duan, J. ,Tang, Y. P. ,Guo, J. M. ,Shang, E. X. ,Zhu, Z. H. ,Wang, T. ,Yang, Y. D. ,Du, B. ,Yu, S. ,Hou, W. L. , Simultaneous determination of gallic acid, protocatechuic acid, catechin, epicatechin, quercetin and kaempferol in Chinese chestnut (Castanea mollissima blume) kernel by high-performance liquid chromatography with diode array detection. Acta Chromatographica Vol. 26, no. 3/2014
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